Mechanical Study of a Chrome-Molybdenum Steel with Hard Coating

Authors

DOI:

https://doi.org/10.46842/ipn.cien.v25n1a10

Keywords:

adherence, boriding, delamination

Abstract

The thermochemical treatment of boron is evaluated at temperatures of 950 and 1000°C, with an exposure time of 2 and 0.5 h; the adhesion of the layer is analyzed using the Rockwell C technique by the German VDI 3198 standard and a qualitative classification is obtained. By optical microscopy the growth and morphology of the FeB/Fe₂B layer on the surface of the material is observed; the presence of FeB/Fe₂B phases was determined by X-ray diffraction (XRD). The scanning electron microscopy (SEM) technique shows the distribution of the alloy elements in the substrate FeB / Fe₂B layer formed on the surface of the medium carbon steel. The elastic modulus and hardness obtained with nanoindentation tests on the generated two-phase layer. The aim of this research is to characterize the morphology, adhesive and mechanical behavior of the boride coating formed on an AISI 4140 steel by means of the dehydrated paste technique, with low diffusion times that prevent the formation of too much of the fragile FeB phase.

References

W. Heinke , A. Leyland , A. Matthews, G. Berg , C. Friedrich, E. Broszeit, “Evaluation of PVD nitride coatings, using impact, scratch and Rockwell-C adhesion tests,” Thin Solid Films, vol. 270, 431-438, 1995.

K. Holmberg, A. Matthews, Properties, “Techniques and Applications in Surface Engineering,” Coatings Tribology, Elsevier Science Press, vol. 56, pp. 65-70, 1994, doi: https://doi.org/10.1016/0040-6090(95)06934-8

A. Meneses Amador, I. Campos Silva, J. Martínez Trinidad, S. Panier, U. Figueroa López, A. Torres Hernández, “An expression to determine the Vickers indentation fracture toughness obtained by the finite element method on Fe.B layers,” Surface and Coatings Technology, vol. 215, pp. 285-290, 2013, doi: https://doi.org/10.1016/j.surfcoat.2012.06.091

N. López Perrusquia, I. Campos Silva, J. Martínez Trinidad, A. Avilés, E. Alvarez Castañeda, S. Juárez Torres, “Evaluation of brittle layers obtained by boriding on AISI H13 steels” Advanced Materials Research, vol. 65, pp. 47-52, 2009, doi: https://doi.org/10.4028/www.scientific.net/AMR.65.47

N. López Perrusquia, M.A. Doñu Ruiz, V.J. Cortés Suarez, L. D. Rosado Cruz, D. Sánchez Huitron, “Study of Surface Hardening to Injectors of Gasoline,” Advanced Materials Research, vol. 538-541, pp. 239-242, 2012, doi: https://doi.org/10.4028/www.scientific.net/AMR.538-541.239

N. López Perrusquia, M. A. Doñu Ruíz, F. Vásquez-Ramírez, O. Trujillo Alfaro, E.Y. Vargas Oliva, “Study of Adhesion in Steels Surface Hardened,” Advanced Materials Research, vol. 535-537, pp. 513-516, 2012, doi: https://doi.org/10.4028/www.scientific.net/AMR.535-537.513

Daimler Benz Adhesion Test, Norma No. 3198, Verein Deutscher Ingenieure (VDI), 1992.

S. Taktak, “Some mechanical properties of borided AISI H13 and 304 steels,” Materials and Design, vol. 28, pp. 1836–1843, 2007, doi: https://doi.org/10.1016/j.matdes.2006.04.017

D. Sanchez Huerta, T. De la Mora Ramírez, M.A. Doñu Ruiz, N. López Perrusquia, J.V. Cortés Suarez, “Characterization of Adherence Steels Hardened Superficially,” MRS Proceedings, vol. 1616, no. S5C, P041, 2013, doi: http://dx.doi.org/10.1557/opl.2014.232

S. Taktak, “Identification of delamination failure of boride layer on common Cr based steels,” Journal of Materials Engineering and Performance, vol. 15, no. 5, pp. 570-574, 2006, doi: https://doi.org/10.1361/105994906X124587

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Published

10-09-2024

How to Cite

Mechanical Study of a Chrome-Molybdenum Steel with Hard Coating. (2024). Científica, 25(1), 1-8. https://doi.org/10.46842/ipn.cien.v25n1a10